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ICPMS daily performance check report, April 16, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040755–000040869

Folder label: “ICPMS 4/16/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08012 Sample Date/Time: Tuesday, April 16,2002 12:15:51 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\newyork city\AE0801 2.572 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 23301.061 1.558 0.044 52.54743 1.13 ug/L > Se-1 45 533191.410 2.190 533191.410 ug/L Cr 52 478003.530 3.003 0.879 45.74843 1.70 ug/L Cr 53 58950.851 2.486 0.109 48.05643 4.23 ug/L Mn 55 949785.023 3.517 1.779 57.96194 1.52 ug/L NI 60 114266.781 0.183 0.214 43.97354 2.37 ug/L Cu 63 285538.254 2.543 0.535 50.61598 0.59 ug/L Cu 65 130986.083 1.853 0.245 44.31622 0.39 ug/L Zn 66 98331.663 1.492 0.955 52.84965 3.88 ug/L Zn 67 16408.970 3.293 0.159 48.54350 0.61 ug/L Zn 68 72509.755 0.726 0.704 52.95786 3.53 ug/L Ge 72 102452.421 2.952 102452.421 ug/L As 75 105490.069 2.789 1.031 49.14245 5.63 ug/L Se 77 11105.807 3.036 0.107 57.01667 5.89 ug/L Se 82 12688.983 3.318 0.123 54.08935 6.09 ug/L Ag 107 490862.551 2.332 0.371 44.56454 4.80 ug/L Cd 111 133979.076 3.844 0.100 48.39595 2.02 ug/L Cd 114 336392.116 1.022 0.254 53.76333 3.58 ug/L > In 115 1323973.446 2.658 1323973.446 ug/L Sb 121 483117.090 1.394 0.365 54.40895 1.32 ug/L Sb 123 355661.823 1.631 0.269 50.09425 1.53 ug/L Ba 135 176173.644 2.861 0.098 64.64236 2.07 ug/L Ba 137 307408.176 0.493 0.171 63.84598 2.92 ug/L > Tb 159 1802793.103 2.392 1802793.103 ug/L Ho 165 1739239.935 1.222 -0.011 ug/L TI 205 1285514.020 1.118 0.712 54.35342 2.38 ug/L Pb 208 1648584.390 1.910 0.913 49.7904.6 1.30 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 105.100 > Sc-1 45 109.096 Cr 52 91.411 Cr 53 95.488 Mn 55 89.898

Sample ID: AE08012 Report Date/Time: Tuesday, April 16, 2002 12:18:49 Page 1

NYC-WTC_000040808

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NYC-WTC_000040808Source: NYC Law Department, mirrored locally

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