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ICPMS daily performance check report, April 16, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040755–000040869

Folder label: “ICPMS 4/16/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08012 Sample Date/Time: Tuesday, April 16, 2002 12:44:35 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\newyork city\AE0801 2.573 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 22135.138 0.912 0.045 54.53223 1.73 ug/L > Se-1 45 488088.850 1.262 488088.850 ug/L Cr 52 441316.938 3.389 0.887 46.16462 4.48 ug/L Cr 53 53845.552 1.434 0.109 47.92519 1.12 ug/L Mn 55 950992.651 2.587 1.947 63.43582 3.76 ug/L Ni 60 107573.123 0.334 0,220 45.21371 1.54 ug/L Cu 63 259768.835 0.824 0.532 50.30876 1.13 ug/L Cu 65 119870.049 3.806 0.245 44.31971 5.11 ug/L Zn 66 91184.541 3.041 0.956 52.91376 2.61 ug/L Zn 67 16049.318 1.728 0.168 51.33224 1.84 ug/L Zn 68 64916.017 2.375 0.680 51.18637 2.51 ug/L > Ge 72 94817.882 0.970 94817.882 ug/L As 75 92632.026 0.734 0.977 46.58103 1.66 ug/L Se 77 10051.319 3.161 0.105 55.67966 2.87 ug/L Se 82 11389.911 0.512 0.119 52.38697 0.46 ug/L Ag 107 462096.478 1.213 0.364 43.73777 2.20 ug/L Cd 111 130245.562 3.676 0.102 49.07493 0.81 ug/L Cd 114 309170.448 1.038 0.244 51.55033 4.39 ug/L > In 115 1269517.077 3.431 1269517.077 ug/L Sb 121 455953.988 0.777 0.359 53.57484 2.88 ug/L Sb 123 340158.265 2.761 0.268 49.96234 0.79 ug/L Ba 135 166577.275 2.609 0.094 62.15857 1.51 ug/L Ba 137 283109.576 1.622 0.160 59.78670 2.24 ug/L > Tb 159 1772372.133 1.102 1772372.133 ug/L Ho 165 1680097.464 2.530 -0.028 ug/L Tl 205 1179301.655 1.566 0.665 50.70183 2.11 ug/L Pb 208 1578975.840 2.021 0.890 48.49603 1.12 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 109.069 > Sc-1 45 99.868 Cr 52 92.243 Cr 53 95.225 Mn 55 100.846

Sample ID: AE08012 Report Date/Time: Tuesday, April 16, 2002 12:47:14 Page 1

NYC-WTC_000040810

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NYC-WTC_000040810Source: NYC Law Department, mirrored locally

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