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GCMS surrogate recovery data for sample AE07765, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07765 analyzed on April 18, 2002.

NYC-WTC_000040279–000040285

Folder label: “GCMS X 4/3/02 A 4/10/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 4 • - Data File : C:\MSDCHEM\l\DATA\020410\05286.D Vial: 12 • * Acq On : 10 Apr 2002 8:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 11 15:55:10 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\1... \SCANAPR0902. M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 11 15:44:30 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.66 152 2555007 20.00 ug/1 -0.01 10) Naphthalene-d8 15.77 136 9646900 20.00 ug/1 -0.02 17) Acenaphthene-diO 23.66 164 5319900 20.00 ug/1 -0.01 31) Phenanthrene-diO 30.90 188 8527264 20.00 ug/1 0.00 39) Chrysene-dl2 39.09 240 6182307 20.00 ug/1 -0.02 45) Perylene-dl2 42.30 264 3023493 20.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 26.73 207 189447 2.97 ug/1 0.17 Spiked Amount 4.000 Recovery = 74.25% 38) 2,4-DDD 0.00 235 0 0.00 ug/ml Spiked Amount 5.000 Recovery 0.00%

Target Compounds Qvalue 36) Di-n-butylphthalate 33.98 149 216686 0.45 ug/1 93

(#) = qualifier out of range (m) = manual integration (+) = signals summed 05286.D SCANAPR0902.M Thu Apr 11 15:55:20 2002 Page 1

NYC-WTC_000040279

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NYC-WTC_000040279Source: NYC Law Department, mirrored locally

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