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GCMS analysis results for sample AE08323, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048106–000048120

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 22 15:38:19 2002 Quant Results File: SCAN020418.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 15:35:07 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 10654857 40.00 ug/1 -0.05 10) Naphthalene-d8 16.54 136 40901955 40.00 ug/1 -0.07 17) Acenaphthene-diO 24.46 164 22353704 40.00 ug/1 -0.06 30) Phenanthrene-dlO 31.72 188 33772332 40.00 ug/1 -0.06 38) Chrysene-dl2 39.94 240 26718286 40.00 ug/1 -0.07 44) Perylene-dl2 43.16 264 20411987 40.00 ug/1 -0.04

System Monitoring Compounds 2 7) TCMX 27.54 207 814695 5.87 ug/1 -0.07 Spiked Amount 8.000 Recovery = 73.38% Target Compounds Qvalue 35) Di-n-butylphthalate 34.81 149 202958 0.17 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08323.D SCAN020418.M Mon Apr 22 15:39:51 2002 Page 1

NYC-WTC_000048108

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NYC-WTC_000048108Source: NYC Law Department, mirrored locally

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