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GCMS analysis results for sample AE08426, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048169–000048181

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048171
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020419\08426.D Vial: 13 Acq On : 19 Apr 2002 7:57 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 22 15:55:08 2002 Quant Results File: SCAN020418.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 08:00:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 10854114 40.00 ug/1 -0.05 10) Naphthalene-d8 16.54 136 41880466 40.00 ug/1 -0.07 17) Acenaphthene-diO 24.46 164 23136992 40.00 ug/1 -0.06 30) Phenanthrene-diO 31.72 188 34787993 40.00 ug/1 -0.06 38) Chrysene-dl2 39.93 240 27064087 40.00 ug/1 -0.08 44) Perylene-dl2 43.16 264 19886440 40.00 ug/1 -0.04

System Monitoring Compounds 27) TCMX 27.54 207 800585 5.57 ug/1 -0.08 Spiked Amount 10.000 Recovery = 55.70% £.0 ‘ 69.6 Target Compounds Qvalue 35) Di-n-butylphthalate 34.81 149 172111 0.14 ug/1 97 43) Bis(2-ethylhexyl)phthalate 40.52 149 50168 0.07 ug/1 77

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08426.D SCAN020418.M Mon Apr 22 15:56:27 2002 Page 1

NYC-WTC_000048171

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NYC-WTC_000048171Source: NYC Law Department, mirrored locally

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