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Document / 11 pages

GCMS analysis results for sample AE08489, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE08489 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048672–000048682

Folder label: “GCMS X 4/10/02 A 4/20/02

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Scanned page image, NYC-WTC_000048674
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020419\08488.D Vial: 25 Acq On : 20 Apr 2002 7:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 26 15:25:58 2002 Quant Results File: SCAN020418.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 08:00:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 9945048 40.00 ug/1 -0.05 10) Naphthalene-d8 16.54 136 37997531 40.00 ug/1 -0.07 17) Acenaphthene-diO 24.46 164 20879523 40.00 ug/1 -0.06 30) Phenanthrene-diO 31.72 188 31208056 40.00 ug/1 -0.06 38) Chrysene-dl2 39.93 240 23738537 40.00 ug/1 -0.08 44) Perylene-dl2 43.15 264 17347549 40.00 ug/1 -0.04

System Monitoring Compounds 27) TCMX 27.54 207 936456 7.22 ug/1 -0.08 Spiked Amount 10.000 Recovery = 72.20% Target Compounds Qvalue 35) Di-n-butylphthalate 34.80 149 84559 0.08 ug/1 98 43) Bis(2-ethylhexyl)phthalate 40.53 149 144642 0.24 ug/1 88

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08488.D SCAN020418.M Fri Apr 26 15:26:38 2002 Page 1

NYC-WTC_000048674

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NYC-WTC_000048674Source: NYC Law Department, mirrored locally

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