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GCMS analysis results for sample AE08427, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048182–000048194

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048184
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020419\08427.D Vial: 14 Acq On : 19 Apr 2002 8:56 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 22 15:57:51 2002 Quant Results File: SCAN020418.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 08:00:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 11232262 40.00 ug/1 -0.05 10) Naphthalene-d8 16.54 136 43379057 40.00 ug/1 -0.07 17) Acenaphthene-diO 24.46 164 23729003 40.00 ug/1 -0.06 30) Phenanthrene-diO 31.72 188 35788649 40.00 ug/1 -0.05 38) Chrysene-dl2 39.94 240 27560229 40.00 ug/1 -0.07 44) Perylene-dl2 43.16 264 20208713 40.00 ug/1 -0.04 System Monitoring Compounds 27) TCMX 27.54 207 821727 5.58 ug/1 -0.08 Spiked Amount 10.000 Recovery = 55.80% c 69.8 Target Compounds Qvalue 35) Di-n-butylphthalate 34.80 149 183406 0.15 ug/1 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08427.D SCAN020418.M Fri Apr 26 14:47:19 2002 Page 1

NYC-WTC_000048184

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NYC-WTC_000048184Source: NYC Law Department, mirrored locally

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