GCMS quantitative results for sample AE07633, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020410\0403REF2.D Vial: 7 Acq On : 10 Apr 2002 4:04 pm Operator: Nefliu Sample : 04/03 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 11 13:59:05 2002 Quant Results File: SCANAPR0902.R

Quant Method : C:\MSDCHEM\l-..\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 14:51:40 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.66 152 2496368 20.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 9404872 20.00 ug/1 -0.01 17) Acenaphthene-dlO 23.66 164 5209756 20.00 ug/1 0.00 31) Phenanthrene-diO 30.90 188 8284224 20.00 ug/1 0.00 39) Chrysene-dl2 39.10 240 6594981 20.00 ug/1 -0.02 45) Perylene-dl2 42.30 264 3339138m 20.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 26.73 207 223186 3.07 ug/1 0.17 Spiked Amount 5.000 Recovery = 61.40% 38) 2,4-DDD 0.00 235 0 0.00 ug/ml Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.65 74 396963m 4.96 ug/1 3) bis(2-Chloroethyl)ether 9.94 93 1291990 8.69 ug/1 97 4) 1.3-Dichlorbenzene 10.41 146 1376551 7.65 ug/1 98 5) 1,4-Dichlorobenzene 10.72 146 1407236 7.75 ug/1 98 6) 1,2-Dichlorobenzene 11.23 146 1359145 7.95 ug/1 98 7) 2,2'oxybis(1-Chloropropane 12.03 45 2199145m 8.75 ug/1 8) N-Nitroso-di-n-propylamine 12.51 43 927337 9.27 ug/1 96 9) Hexachloroethane 12.52 119 479962 7.85 ug/1 95 11) Nitrobenzene 12.92 77 1285443 8.05 ug/1 99 12) 1sophorone 14.03 82 2214037 8.17 ug/1 100 13) bis(2-Chloroethoxy) methan 15.25 93 1598985 9.17 ug/1 98 14) 1,2,4-Trichlorobenzene 15.62 180 1160830 8.52 ug/1 98 15) Naphthalene 15.85 128 4077484 9.00 ug/1 100 16) Hexachlorobutadiene 16.62 225 626134 8.41 ug/1 98 18) Hexachlorocyclopentadiene 19.79 237 67502 1.47 ug/1 88 19) 2-Chloronaphthalene 21.13 162 2418109 8.46 ug/1 100 20) Acenaphthylene 22.95 152 3495354 8.75 ug/1 99 21) Dimethyl phthalate 23.04 163 3003520 9.63 ug/1 99 22) 2,6-Dinitrotoluene 23.15 77 158667 9.51 ug/1 # 80 23) Acenaphthene 23.79 153 2628089 8.93 ug/1 99 24) 2,4-Dinitrotoluene 24.92 165 524835 6.97 ug/1 96 25) Fluorene 26.20 166 2921713 9.04 ug/1 100 26) Diethyl phthalate 26.41 149 3007665 9.89 ug/1 98 27) 4-Chlorophenyl-phenylether 26.53 204 1378919 9.10 ug/1 96 29) N-Nitrosodiphenylamine 27.13 168 923922 7.57 ug/1 98 30) Azobenzene 27.21 77 3117158 8.65 ug/1 98 32) Hexachlorobenzene 28.77 284 932804 8.57 ug/1 98 33) 4-Bromophenyl-phenylether 28.89 248 787083 8.83 ug/1 96

(#) = qualifier out of range (m) = manual integration 0403REF2.D SCANAPRO902.M Thu Apr 11 14:00:28 2002 Page 1

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