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GCMS reference results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Reference analysis report listing detected compounds and their concentrations for sample AE06991 analyzed on April 6, 2002.

NYC-WTC_000040052–000040059

Folder label: “GCMS X 3/26/02 A 4/6/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO4O5\REFA1.D Vial: 17 Acq On 6 Apr 2002 8:42 am Operator: Sample gc/ms scan 3/26 Inst : GC/MS 2 09 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 15 14:24 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 15 14:10:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.73 284 119641 22.78 ug/1 98 34) Phenanthrene 25.70 178 513784 22.58 ug/1 100 35) Anthracene 25.83 178 459347 20.80 ug/1 100 36) Di-n-butylphthalate 27.60 149 652158 23.82 ug/1 100 37) Fluoranthene 29.33 202 468842 21.10 ug/1 97 40) Pyrene 30.00 202 490498 24.16 ug/1 99 41) Butylbenzylphthalate 32.13 149 195685 22.32 ug/1 99 42) Benzo(a)anthracene 33.64 228 267547 21.74 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.91 149 241004 23.93 ug/1 98 44) Chrysene 33.76 228 295220 23.75 ug/1 99 46) Di-n-Octylphthalate 35.65 149 248241 18.36 ug/1 # 99 47) Benzo(b)fluoranthene 36.74 252 196729 20.98 ug/1 99 48) Benzo(k)fluoranthene 36.81 252 229409 23.71 ug/1 99 49) Benzo(a)pyrene 37.73 252 133628 17.58 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.05 276 130261 18.84 ug/1 98 51) Dibenz(a,h)anthracene 42.12 278 106796 19.80 ug/1 99 52) Benzo(g,h,i)perylene 43.29 276 117774 20.82 ug/1 100

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0408.M Mon Apr 15 14:26:29 2002 Page 2

NYC-WTC_000040055

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NYC-WTC_000040055Source: NYC Law Department, mirrored locally

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