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GCMS calibration data for sample AE05847, April 16 2002

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Calibration report listing detector response values and minimum detection levels for various organic compounds analyzed on April 16, 2002.

NYC-WTC_000059603–000059607

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO 3 0 2 2\REFA.D Vial: 16 Acq On 4 Apr 2002 10:28 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 9 15:20 2002 Quant Results File: GCMS0408.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response' via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.72 284 97716 17.60 ug/1 95 34) Phenanthrene 25.69 178 481886 20.04 ug/1 99 35) Anthracene 25.83 178 428029 18.33 ug/1 100 36) Di-n-butylphthalate 27.60 149 2508716 86.71 ug/1 100 37) Fluoranthene 29.32 202 450926 19.20 ug/1 99 40) Pyrene 30.00 202 463592 21.55 ug/1 98 41) Butylbenzylphthalate 32.13 149 191192 20.58 ug/1 99 42) Benzo(a)anthracene 33.64 228 253207 19.42 ug/1 98 43) Bis(2-ethylhexyl)phthalate 33.90 149 248012 23.24 ug/1 99 44) Chrysene 33.76 228 281162 21.35 ug/1 99 46) Di-n-Octylphthalate 35.65 149 237662 17.41 ug/1 # 98 47) Benzo(b)fluoranthene 36.74 252 197962 20.91 ug/1 98 48) Benzo(k)fluoranthene 36.81 252 ■ 207883 21.28 ug/1 98 49) Benzo(a)pyrene 37.73 252 125216 16.31 ug/1 97 50) Indeno(1,2,3-cd)pyrene 42.04 276 116499 16.69 ug/1 95 51) Dibenz(a,h)anthracene 42.13 278 99128 18.20 ug/1 98 52) Benzo(g,h,i)perylene 43.27 276 105899 18.53 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA.D GCMS0408.M Tue'Apr 16 08:02:33 2002 Page 2

NYC-WTC_000059606

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NYC-WTC_000059606Source: NYC Law Department, mirrored locally

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