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GCMS calibration results for sample AE06430, April 2002

Machine-extracted title · confidence 100%

Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.

NYC-WTC_000039441–000039444

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR17O2\CAL2O .D Vial: 2 Acq On 17 Apr 2002 9:10 am Operator: Sample Inst : 209 Miso Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 15:32 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 195796 22.30 ug/1 95 34) Phenanthrene 25.66 178 813191 20.60 ug/1 100 35) Anthracene 25.79 178 792327 20.40 ug/1 99 36) Di-n-butylphthalate 27.56 149 947142 19.18 ug/1 100 37) Fluoranthene 29.28 202 804189 20.25 ug/1 97 4 0) Pyrene 29.95 202 819951 20.58 ug/1 96 41) Butylbenzylphthalate 32.08 149 345881 17.75 ug/1 95 42) Benzo(a)anthracene 33.59 228 543233 19.65 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 422832 16.96 ug/1 98 44) Chrysene 33.72 228 555734 20.27 ug/1 99 46) Di-n-Octylphthalate 35.60 149 582213 / 14.96 ug/l 99 47) Benzo(b)fluoranthene 36.69 252 478823 —19.04 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 485864 19.84 ug/1 97 49) Benzo(a)pyrene 37.68 252 395809 19.09 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.95 276 421862 20.21 ug/1 96 51) Dibenz(a,h)anthracene 42.03 278 324050 20.36 ug/1 97 52) Benzo(g,h,i)perylene 43.17 276 362679 20.81 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL20.D GCMS0412.M Wed Apr 17 15:33:37 2002 Page 2

NYC-WTC_000039443

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NYC-WTC_000039443Source: NYC Law Department, mirrored locally

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