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GCMS analysis results for sample AE02093, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02093 conducted on March 20, 2002, showing surrogate compound data.

NYC-WTC_000038941–000038948

Folder label: “GCMS X 3/8/02 A 3/19/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031802\2093.D Vial: 20 Acq On : 19 Mar 2002 5:43 pm Operator: McLean Sample : GC/MS SCAN 3/8 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.543 708 713 736 rBV 1604336 5001314 64.09% 12.393% 2 13.017 1091 1096 1120 rBV 3198047 7144797 91.56% 17.705% 3 18.133 1654 1660 1676 rBV 3836808 7671651 98.31% 19.010% 4 22.496 2134 2141 2155 rBV2 3271024 7803212 100.00% 19.336% 5 27.430 2681 2685 2696 rBV 512977 1033187 13.24% 2.560%

6 30.305 2995 3002 3019 rBV2 3067195 7398907 94.82% 18.334% 7 34.178 3422 3429 3453 rBV 1704997 4302246 55.13% 10.661%

Sum of corrected areas: 40355314

2093.D 5080302.M Wed Mar 20 02:15:00 2002 Page 1

NYC-WTC_000038946

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NYC-WTC_000038946Source: NYC Law Department, mirrored locally

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