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GCMS analysis results for sample AE01440, Feb 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated February 22, 2002.

NYC-WTC_000038623–000038631

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB2102\1440.D Vial: 12 •Acq On : 22 Feb 2002 12:56 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.328 789 794 807 rVB 580549 1444576 15.72% 5.987% 2 15.973 1185 1191 1207 rBV 930615 1886769 20.54% 7.819% 3 21.288 1763 1770 1784 rBV 1006341 2058050 22.40% 8.529% 4 25.732 2248 2254 2265 rBV2 911658 1907741 20.76% 7.906% 5 27.494 2435 2446 2465 rBV 621410 1555972 16.94% 6.449%

6 29.881 2695 2706 2738 rBV 1042465 3218550 35.03% 13.339% 7 30.808 2802 2807 2814 rVB 137985 276510 3.01% 1.146% 8 33.801 3126 3133 3150 rBV2 629633 1436112 15.63% 5.952% 9 36.289 3395 3404 3435 rBV 3587760 9187557 100.00% 38.077% 10 38.079 3591 3599 3612 rBV2 382813 1157341 12.60% 4.796%

Sum of corrected areas: 24129178

1440.D GCMS0308.M Mon Mar 25 08:22:23 2002

NYC-WTC_000038626

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NYC-WTC_000038626Source: NYC Law Department, mirrored locally

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