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GCMS quantitation results for sample AE04032, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038552–000038561

Folder label: “GCMS X 2/25/02 A 3/23/02

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OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAR2202\4032.D Vial: 38 -Acq On : 24 Mar 2002 6:35 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.263 781 786 801 rVB 1070764 2414677 61.15% 12.581% 2 14.861 1064 1069 1074 rVB 112016 211858 5.37% 1.104% 3 15.898 1176 1182 1198 rBV 1659408 3447689 87.31% 17.963% 4 21.214 1754 1761 1776 rBV 1904406 3948654 100.00% 20.573% 5 25.657 2238 2245 2256 rBV2 1841352 3864216 97.86% 20.133%

6 25.795 2257 2260 2272 rVB2 15345 45220 1.15% 0.236% 7 27.622 2454 2459 2465 rBV 50200 96036 2.43% 0.500% 8 30.725 2792 2797 2803 rBV 192533 394256 9.98% 2.054% 9 33.717 3116 3123 3141 rBV2 1196852 2727060 69.06% 14.208% 10 33.929 3141 3146 3152 rBV 80299 165464 4.19% 0.862%

11 37.968 3577 3586 3603 rBV2 633825 1878444 47.57% 9.787%

Sum of corrected areas: 19193574

4032.D GCMS0308.M Tue Mar 26 10:45:16 2002

NYC-WTC_000038557

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NYC-WTC_000038557Source: NYC Law Department, mirrored locally

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