NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
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GCMS analysis results for sample AE01440, Feb 2002
Machine-extracted title · confidence 100%Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated February 22, 2002.
NYC-WTC_000038623–000038631Folder label: “GCMS X 2/25/02 A 3/23/02”
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NYC 9/11 Public Portal Document
:* Data File : C:\HPCHEM\1\DATA\FEB2102\1440.D Vial: 12 4 Acq On : 22 Feb 2002 12:56 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 9:182002 ।Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 251262 20.00 ug/1 -0.03 10) Naphthalene-d8 15.97 136 959963 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.29 164 523437 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.73 188 720188 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 468057 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 331531 20.00 ug/1 -0.04
System Monitoring Compounds 37) 2,4-DDD 30.81 235 51160 6.14 ug/mL 0.31 Spiked Amount 5.000 Recovery = 122.80% I
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00- 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 198 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.76 149 912 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1440.D GCMS0308.M Mon Mar 25 08:21:12 2002 Page 1
NYC-WTC_000038623
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NYC-WTC_000044723
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Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
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Calibration scan report for EPA Method 625 showing retention times and deviations for deuterated standards on April 25 2002.
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Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044700
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003803
GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052630
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
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