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GCMS quantitation results for sample AE03471, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038458–000038464

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\022802\03471.D Vial: 20 Acq On 1 Mar 2002 4:08 am Operator: McLean * Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.579 712 717 736 rBV 1904359 4763769 67.53% 12.334% 2 12.083 988 993 998 rVB 279163 454673 6.45% 1.177% 3 13.053 1095 1100 1114 rBV 3468181 6460132 91.58% 16.726% 4 18.160 1657 1663 1675 rBV 3625907 7006944 99.33% 18.142% 5 22.522 2138 2144 2158 rBV2 3373667 7053903 100.00% 18.263%

6 27.457 2683 2688 2698 rBV 623030 1111923 15.76% 2.879% 7 30.332 2998 3005 3025 rBV2 3084856 6675366 94.63% 17.283% 8 30.940 3067 3072 3083 rBV 211313 452574 6.42% 1.172% 9 34.205 3425 3432 3452 rBV2 1938634 4643706 65.83% 12.023%

Sum of corrected areas: 38622990

33471.D 5080202.M Wed Mar 13 06:54:42 2002 Page 1

NYC-WTC_000038461

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NYC-WTC_000038461Source: NYC Law Department, mirrored locally

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