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GCMS analysis results for sample AE01913 with surrogate data, Mar

Machine-extracted title · confidence 50%

Laboratory report for sample AE01913 showing GCMS analysis of unknown compounds and surrogate recovery on March 7, 2002.

NYC-WTC_000003964–000003971

Folder label: “GCMS X 1/28/02 A 2/25/02

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Scanned page image, NYC-WTC_000003969
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NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\DATA\022502\1913 .D Vial: 37 Acq On : 25 Feb 2002 7:43 pm Operator: McLean Sample : SAMPLE 1913 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.579 712 717 734 rBV 1983430 4852108 69.48% 12.568% 2 13.053 1095 1100 1115 rBV 3483353 6455212 92.43% 16.721% 3 18.160 1657 1663 1674 rBV 3371635 6792621 97.27% 17.595% 4 22.523 2138 2144 2158 rBV2 3353885 6944597 99.44% 17.988% 5 22.677 2158 2161 2172 rVB2 26333 79529 1.14% 0.206%

6 27.457 2684 2688 2699 rVB 533212 950777 13.61% 2.463% 7 30.341 2999 3006 3026 rBV2 2947638 6983585 100.00% 18.089% 8 34.214 3425 3433 3450 rBV 2315279 5547603 79.44% 14.370%

Sum of corrected areas: 38606032

13.D 5080202.M Wed Feb 27 09:02:51 2002 Page 1

NYC-WTC_000003969

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NYC-WTC_000003969Source: NYC Law Department, mirrored locally

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