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GCMS quantitation results for sample AE03440, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038440–000038448

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\022802\03440.D Vial: 27 . Acq On 1 Mar 2002 9:53 am Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.579 712 717 738 rBV 2038174 5059815 68.33% 12.521% 2 12.083 988 993 997 rBV 307504 502725 6.79% 1.244% 3 13.053 1095 110.0 1115 rBV 3696321 6870271 92.77% 17.001% 4 18.160 1657 1663 1682 rBV 3763167 7405375 100.00% 18.325% 5 22.523 2138 2144 2158 rBV2 3532176 7385984 99.74% 18.277%

6 22.677 2158 2161 2171 rVB2 26431 75731 1.02% 0.187% 7 27.457 2683 2688 2694 rBV 635478 1106399 14.94% 2.738% 8 30.332 2998 3005 3027 rBV2 3080978 6650299 89.80% 16.456% 9 30.940 3067 3072 3082 rBV 203319 455196 6.15% 1.126% 10 34.205 3425 3432 3456 rBV2 2035273 4899653 66.16% 12.124%

Sum of corrected areas: 40411448

03440.D 5080202.M Wed Mar 13 06:51:06 2002 Page 1

NYC-WTC_000038445

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NYC-WTC_000038445Source: NYC Law Department, mirrored locally

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