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GCMS quantitation results for sample AE03454, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038405–000038413

Folder label: “GCMS X 2/26/02 A 2/28/02

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Data File C:\MSDCHEM\l\DATA\022802\03454FB.D Vial: 29 • Acq On 1 Mar 2002 11:32 am Operator: McLean Sample MS CSAN FB Q Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.81 ug/L 614803 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclopentasiloxane, decamethyl- 37G C10H3005Si5 000541-02-6 74 2 N-(Trifluoroacetyl)-N, 0,0',O''-t... 553 C22H42F3NO4Si4 000000-00-0 47 3 Benzeneethanamine, N-[(pentafluo. . . 563 C24H34F5NO3Si3 055429-13-5 43 4 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 43 Abundance Scan 993 (12.083 min): 03454FB.D (-) m/z 73.10 100.00% 73

5000 267 355

— —r ! • i «I r ■ 11.8012.0012.2012.40 0- +108.154.12223 TITr 323 1111 T m/z 267.00 46.57% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyc lope asilo xane, decamethyl- 73

5000 267 -r-r-rr-r-n-f • I ‘ ' ■ I ‘ ' 11.80 12.00 12.20 12.40 355 m/z 355.10 38.98%

28 i 1 103133163193223 x 0+ — —Trmtr ■ 1323 1r I 111111 T 1’t miz-> 50 100 150 200 250 300 350 460 450 500 550 Abundance #377151: N-(T rifluoroacety!)-N,O,0 ’.0"tetrakis(trimethyl... 73 — — 355 11.80 12.00 12.20 12.40 5000 m/z 356.10 13.91%

.. , 1161*7 193- .. 236267 ........................................................................................ —-- - - 538 TTpBfrf I------ .... 1.. ri ।।1111 > । > miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 I * * ‘ ' I 11I T 355 11.80 12.00 12.20 12.40 m/z 268.00 11.95%

5000

0- -44+4 mmmmmemmmmm 117147177207 251281 386 458 548 m/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40 )3454FB.D 5080202.M Wed Mar 13 06:53:26 2002 Page 3

NYC-WTC_000038412

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NYC-WTC_000038412Source: NYC Law Department, mirrored locally

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