GCMS analysis results for sample AE03915, Mar 18 2002

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Laboratory report documenting GCMS analysis of sample AE03915 for unknown compounds on March 18, 2002.

NYC-WTC_000038342–000038351

Folder label: “GCMS X 2/22/02 A 2/24/02”

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NYC 9/11 Public Portal Document ■ . . Library Search Compound Report

Data File : C : \HPCHEM\ DATA FEB2 1023915.D Vial: 77 Acq On : 24 Feb 2002 9:47 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-diO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.87 0.23 ug/1 16135 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- C 001719-06-8 64 188 C14D10 2 Phenanthrene-dl0 001517-22-2 38 188 C14D10 3 Quinazoline, 4-(1-methylethyl)-, 1- 188 C11H12N2O 050915-32-7 9 4 4-Me thy J/-2-(4-fluorophenyl) pyrimidi 188 C11H9FN2 076128-67-1 9 Abundance Scan 2269 (25.869 min): 3915.D (-) m/z 188.10 100.00% 168

5000 80 y i 94 158 TT ' 1 I 1 1 1 1 I 1 1 66 25.60 25.80 26.00 26.20 i 44 TTT ' ' । ' ' ' ' । । । । ' I । । 11 I 1 11111 Trt ' ' I’*' ' l‘ ‘ ' 1 | ' * ♦ • | • p । • । | • । । I | i « . < | r ( m/z 79.95 38.49% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ‘Abundance #19957: Anthracene-d10- 188

5000 — P . .... — 25.60 25.80 26.00 26.20 80 94 . m/z 189.05 19.44% 66 160 ■ i • ■ • ■ i ■ •' ■ i ■ ■ ■ • i • 1 .1 i'' ■ ■ i ■ ■'' i''' ■ i I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958; Phenanthrene-d10 188 -................... 25.60 25.80 26.00 26.20 5000 m/z 184.10 18.43%

80 94 160 66 । 1 11'1' * 11 *1' ।'''' ।1 ■ | t • ' | » t ■ ■ • • i • • ■ ■ । ■ ■ ■ ■ । ■11 • ■ ■ ■ । i ■ ■ ■ ■ i'' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19875: Quinazoline, 4-(1 -methylethyl)-, 1-oxide ‘I 188 25.60 25.80 26.00 26.20 1 m/z 9 . 00 18.04% । 173 5000

157

'm/z-> ' I ' " ................. i i I I | ri ri | i i > i |T 40 50 60 70 80 90 —lI 117 131 146 100 110 120 130 140 150 160 170 180 190 1 — TT’ 25.60 25.80 26.00 26.20

3915.D GCMS0208.M Wed Mar 13 11:37:05 2002 Page 2

NYC-WTC_000038350

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GCMS analysis results for sample AE03916, Mar 15 2002 · Box DEP Box 23

NYC-WTC_000038292

Laboratory report documenting GCMS analysis of sample AE03916 conducted on March 15, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999