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GCMS analysis results for sample AE04027, Mar 18 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE04027 for unknown compounds on March 18, 2002.

NYC-WTC_000038334–000038341

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038338
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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\FEB2102\4027.D Vial: 82 Acq On : 25 Feb 2002 2:41 am Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.203 339 344 360 rBV 49700 193126 13.68% 2.714% 2 12.334 788 794 811 rBV 335296 1022641 72.42% 14.372% 3 15.970 1184 1190 1208 rBV 614941 1331786 94.31% 18.716% 4 21.285 1763 1769 1790 rBV 667770 1412126 100.00% 19.845% 5 25.728 2247 2253 2266 rBV2 600069 1295631 91.75% 18.208%

6 30.805 2802 2806 2812 rVB 88354 180568 12.79% 2.538% 7 33.798 3126 3132 3152 rBV2 424819 994781 70.45% 13.980% 8 38.076 3590 3598 3613 rBV2 209789 685081 48.51% 9.628%

Sum of corrected areas: 7115740

4027.D GCMS0208.M Wed Mar 13 11:41:23 2002

NYC-WTC_000038338

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NYC-WTC_000038338Source: NYC Law Department, mirrored locally

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