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GCMS analysis results for sample AD31590, Feb 28 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31590 conducted on February 28, 2002.

NYC-WTC_000038187–000038195

Folder label: “GCMS X 2/21/02 A 2/22/02

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Scanned page image, NYC-WTC_000038192
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB2102\31590.D Vial: 40 Acq On : 23 Feb 2002 5:34 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.203 339 344 358 rBV 129413 350060 14.38% 2.825% 2 12.334 788 794 807 rVB 684330 1719815 70.63% 13. 879% 3 15.970 1184 1190 1209 rBV 1042171 2225540 91.39% 17.960% 4 21.285 1763 1769 1784 rBV 1169127 2435083 100.00% 19.652% 5 25.737 2247 2254 2264 rBV2 1057053 2278579 93.57% 18.389%

6 30.814 2802 2807 2813 rBV 165960 335238 13.77% 2.705% 7 33.807 3125 3133 315.0 rBV 734132 1711313 70.28% 13.811% 8 38.085 3590 3599 3616 rBV2 434665 1335682 54.85% 10.779%

Sum of corrected areas: 12391310

31590.D GCMS0208.M Wed Feb 27 12:04:32 2002

NYC-WTC_000038192

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NYC-WTC_000038192Source: NYC Law Department, mirrored locally

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