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GCMS analysis results for sample AE01439, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01439 analyzed via GCMS on March 6, 2002, including surrogate recovery data.

NYC-WTC_000009897–000009905

Folder label: “GCMS X 1/22/02 A 2/22/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘Data File : C:\HPCHEM\l\DATA\FEB2102\1439.D Vial: 11 Acq On : 21 Feb 2002 11:57 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.207 342 345 350 rBV 9274 19597 1.03% 0.215% 2 12.329 789 794 810 rVB 561119 1358002 71.17% 14.901% 3 15.973 1185 1191 1204 rBV 884031 1779317 93.25% 19.524% 4 21.289 1763 1770 1777 rBV 934935 1908122 100.00% 20.937% 5 25.732 2248 2254 2264 rBV2 806606 1748489 91.63% 19.186%

6 30.809 2802 2807 2813 rBV 87844 167245 8.76% 1.835% 7 33.801 3125 3133 3150 rBV2 537215 1220679 63.97% 13.394% 8 38.079 3592 3599 3620 rBV 295080 912113 47.80% 10.008%

Sum of corrected areas: 9113564

1439.D GCMS0208.M Fri Feb 22 09:33:11 2002

NYC-WTC_000009899

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NYC-WTC_000009899Source: NYC Law Department, mirrored locally

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