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GCMS analysis results for sample AE01442, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01442 analyzed via GCMS on March 6, 2002, including surrogate recovery data.

NYC-WTC_000009906–000009914

Folder label: “GCMS X 1/22/02 A 2/22/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\FEB2102\1442.D Vial: 14 Acq On : 22 Feb 2002 2:54 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.203 341 344 351 rBV 10645 25531 1.32% 0.272% 2 12.334 788 794 810 rVB 582489 1399699 72.29% 14.903% 3 15.969 1184 1190 1203 rBV 861296 1823317 94.17% 19.413% 4 21.285 1763 1769 1787 rBV 952725 1936297 100.00% 20.616% 5 25.737 2247 2254 2265 rBV2 828483 1800*813 93.00% 19.173%

6 30.814 2802 2807 2812 rVB 110795 212487 10.97% 2.262% 7 33.797 3125 3132 3146 rBV2 550192 1261973 65.17% 13.436% 8 38.076 3589 3598 3620 rBV2 292721 932200 48.14% 9.925%

Sum of corrected areas: 9392317

1442 .D GCMS0208.M Fri Feb 22 09:36:24 2002

NYC-WTC_000009911

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NYC-WTC_000009911Source: NYC Law Department, mirrored locally

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