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GCMS analysis results for sample AE03833, Mar 15 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE03833 conducted on March 15, 2002.

NYC-WTC_000038273–000038281

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038278
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NYC 9/11 Public Portal Document LSC Area Percent Report

.. Data File : C:\HPCHEM\1\DATA\FEB2102\3833.D Vial: 73 Acq On : 24 Feb 2002 5:52 pm Operator: Sample .: gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak, R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.194 339 343 368 rBV 106664 305338 17.36% 3.322% 2 12.325 789 793 811 rVB 503139 1274128 72.45% 13.864% 3 15.970 1184 1190 1208 rBV 785942 1657465 94.25% 18.035% 4 21.285 1763 1769 1790 rBV 853969 1758536 100.00% 19.135% 5 25.728 2247 2253 2265 rBV2 724745 1651598 93.92% 17.971%

6 30.814 2802 2807 2813 rVB 113972 232305 13.21% 2.528% 7 33.798 3126 3132 3152 rBV2 560139 1313229 74.68% 14.289% 8 38.076 3590 3598 3614 rBV2 318246 997680 56.73% 10.856%

Sum of corrected areas: 9190279

3833.D GCMS0208.M Wed Mar 13 11:32:44 2002

NYC-WTC_000038278

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NYC-WTC_000038278Source: NYC Law Department, mirrored locally

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