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GCMS analysis results, sample AE03616, March 2002

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.

NYC-WTC_000037780–000037799

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

4 Quantitation Report (Not Reviewed) . Data File : C:\MSDCHEM\1\5973N\02MAR08\03516.D Vial: 6 Acq On : 8 Mar 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 15 10:05:20 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP022102

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 2160885 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 9183648 20.00 ug/L 0.00 17) Acenaphthene-diO 18.33 164 4552953 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 7369463 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 5966068 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 4032108 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 474811 4.83 ug/L 0.00 Spiked Amount 5.000 Recovery = 96.60% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 717438 2.60 ug/L # 58 21) 2,6-Dinitrotoluene 18.33 165 581525 9.12 ug/L # 27

(#) = qualifier out of range (m) = manual integration 03516.D HP022102.M Fri Mar 15 10:05:21 2002 Page 1

NYC-WTC_000037782

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NYC-WTC_000037782Source: NYC Law Department, mirrored locally

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