Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed)
Data File : C:\MSDCHEM\1\5973N\02MAR08\03616.D Vial: 6
Acq On : 8 Mar 2002 7:42 pm Operator:
Sample : 508 scan Inst : Instrumen
Mise : March 8, 2002 Multiplr: 1.00
MS Integration Params: SPLIT.P
Quant Time: Mar 15 10:05 2002 Quant Results File: HP022102.R
Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator)
Title : 508 scan method
Last Update : Mon Feb 25 10:47:59 2002
Response via : Initial Calibration
Abundance TIC: 03516.D
1.05e+07
1e+07
3
9500000
2 It
9000000
1
8500000
8000000
7500000
t
i
I I of
I
i 6
7000000 I
6500000-
of
6000000 ]
5500000-
I
5000000
4500000
4000000
3500000
3000000
2500000
C
2000000 §—
N
1500000-
1000000
500000
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Time—> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00
03516.D HP022102.M Fri Mar 15 10:05:22 2002 Page 2
NYC-WTC_000037783
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NYC-WTC_000037783Source: NYC Law Department, mirrored locally
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.