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GCMS blank results for sample AE03614, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.

NYC-WTC_000037740–000037759

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037742
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

* Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 15 10:05:17 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP022102

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1677758 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 7197650 20.00 ug/L 0.00 17) Acenaphthene-diO 18.33 164 3617517 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 6142924 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 4696576 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 2851397 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 355225 4.34 ug/L 0.00 Spiked Amount 5.000 Recovery = 86.80% Target Compounds Qvalue 20) Dimethylphthalate 18.33 163 575558 2.62 ug/L # 58 21) 2,6-Dinitrotoluene 18.33 165 459689 9.07 ug/L # 27

(#) = qualifier out of range (m) = manual integration 03514.D HP022102.M Fri Mar 15 10:05:18 2002 Page 1

NYC-WTC_000037742

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NYC-WTC_000037742Source: NYC Law Department, mirrored locally

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