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GCMS analysis results, sample AE02718, March 2002

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.

NYC-WTC_000010967–000010986

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\l\5973N\02FEB28\02718.D Vial: 3 Acq On : 28 Feb 2002 4:20 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 01 09:02:57 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.72 152 1378279 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 5973201 20.00 ug/L 0.00 17) Acenaphthene-diO 18.34 164 2971117 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 5193287 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 3868162 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 2499584 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 335699 4.85 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.00% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 475920 2.64 ug/L # 57 21) 2,6-Dinitrotoluene 18.33 165 378401 9.09 ug/L # 27

(#) = qualifier out of range (m) = manual integration 02718.D HP022102.M Fri Mar 01 09:02:58 2002 Page 1

NYC-WTC_000010969

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NYC-WTC_000010969Source: NYC Law Department, mirrored locally

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