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GCMS analysis report for sample AE01547, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010066–000010085

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\l\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 25 10:49:12 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1434130 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 6240428 20.00 ug/L 0.00 17) Acenaphthene-diO 18.34 164 3143675 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 5606293 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 4013157 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 2533000 20.00 ug/L -0.04

System Monitoring Compounds 37) 2,4-DDD 27.72 235 294929 3.95 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.00%

Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 511561 2.68 ug/L # 57 21) 2,6-Dinitrotoluene 18.33 165 400578 9.10 ug/L # 27

(#) = qualifier out of range (m) = manual integration 01547.D HP022102.M Mon Feb 25 10:49:13 2002 Page 1

NYC-WTC_000010068

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NYC-WTC_000010068Source: NYC Law Department, mirrored locally

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