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GCMS blank analysis results for sample AD29926, Jan 2002

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Blank quality control analysis for gas chromatography-mass spectrometry, completed January 30, 2002, measuring multiple semi-volatile organic compounds below method detection…

NYC-WTC_000037367–000037374

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1401\LBE.D Vial: 41 Acq On 16 Dec 2001 5:47 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.596 274 278 296 rBV 273435 831274 14.65% 2.914% 2 11.672 717 722 747 rBV 1538608 4103160 72.31% 14.382% 3 15.271 1109 1114 1133 rBV 2224249 5288454 93.20% 18.537% 4 20.549 1683 1689 1713 rBV 2584536 5674122 100.00% 19.889% 5 24.974 2164 2171 2184 rBV2 2253967 5233616 92.24% 18.345%

6 30.051 2719 2724 2731 rBV 280731 570857 10.06% 2.001% 7 33.007 3039 3046 3067 rBV2 1618098 3878829 68.36% 13.596% 8 37.101 3484 3492 3519 rBV2 967288 2949173 51.98% 10.337%

Sum of corrected areas: 28529485

LBE.D GCMSH26.M Wed Jan 30 12:47:22 2002

NYC-WTC_000037371

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NYC-WTC_000037371Source: NYC Law Department, mirrored locally

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