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GCMS sample analysis report for AD29928, Jan 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for environmental sample AD29928 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037448–000037456

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29927.D Vial: 52 Acq On : 16 Dec 2001 4:28 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.602 275 279 292 rBV 198609 579675 9.91% 2.033% 2 11.669 717 722 749 rBV 1497440 4184461 71.52% 14.678% 3 15.277 1109 1115 1134 rBV 2296451 5276348 90.18% 18.508% 4 20.556 1683 1690 1719 rBV 2516360 5850770 100.00% 20.522% 5 24.971 2165 2171 2185 rBV2 2193702 5237747 89.52% 18.372%

6 30.048 2719 2724 2734 rBV 313836 , 680218 11.63% 2.386% 7 33.004 3040 3046 3070 rBV2 1552380 3890333 66.49% 13.646% 8 37.099 3484 3492 3509 rBV 929090 2809572 48.02% 9.855%

Sum of corrected areas: 28509124

29927.D GCMS1126.M Wed Jan 30 11:50:50 2002

NYC-WTC_000037453

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NYC-WTC_000037453Source: NYC Law Department, mirrored locally

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