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GCMS sample analysis report for AD29965, Jan 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for environmental sample AD29965 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037485–000037495

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\1\DATA\DEC1401\29965.D Vial: 49 Acq On : 16 Dec 2001 1:33 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 313 rVB 311715 960125 14.87% 2.943% 2 11.357 685 688 693 rBV 29986 75947 1.18% 0.233% 3 11.440 693 697 705 rVB 27526 81789 1.27% 0.251% 4 11.669 717 722 747 rBV 1803118 4732158 73.27% 14.506% 5 15.277 1109 1115 1136 rBV 2588011 5965763 92.37% 18.288%

6 20.547 1683 1689 1712 rBV 2792664 6458335 100.00% 19.798% 7 24.972 2165 2171 2185 rBV2 2510182 5897403 91.31% 18.079% 8 30.048 2719 2724 2736 rBV 333182 701164 10.86% 2.149% 9 33.005 3040 3046 3073 rBV2 1778282 4459290 69.05% 13.670% 10 37.099 3484 3492 3517 rBV 1138007 3289082 50.93% 10.083%

Sum of corrected areas: 32621056

29965.D GCMS1126.M Wed Jan 30 12:46:42 2002

NYC-WTC_000037490

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NYC-WTC_000037490Source: NYC Law Department, mirrored locally

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