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GCMS analysis results for sample AD30015, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD30015 conducted on January 28, 2002.

NYC-WTC_000037289–000037300

Folder label: “GCMS X 12/11/01 A 12/18/01

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Scanned page image, NYC-WTC_000037294
OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\DEC1801\30015.D Vial: 12 Acq On : 19 Dec 2001 2:50 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title :.209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 291 rBV 350380 946202 12.57% 2.470% 2 7.741 291 294 311 rVB2 44481 177393 2.36% 0.463% 3 11.441 693 697 717 rVB 27228 113950 1.51% 0.297% 4 11.670 717 722 747 rBV 2086851 5534557 73.50% 14.448% 5 15.278 1109 1115 1134 rBV 3098424 6990677 92.84% 18.249%

6 20.557 1683 1690 1712 rBV 3289886 7530068 100.00% 19.658% 7 24.973 2165 2171 2184 rBV2 2983984 6962011 92.46% 18.175% 8 25.119 2185 2187 2199 rVB2 27726 90866 1.21% 0.237% 9 30:049 2719 2724 2736 rBV 365914 788015 10.46% 2.057% 10 33.014 3040 3047 3070 rBV2 2172518 5262626 69.89% 13.738%

11 37.109 3485 3493 3512 rBV 1286947 3909960 51.92% 10.207%

Sum of corrected areas: 38306325

30015.D GCMS1126.M Tue Jan 15 15:37:25 2002

NYC-WTC_000037294

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NYC-WTC_000037294Source: NYC Law Department, mirrored locally

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