Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
NYC-WTC_000034908–000034918Folder label: “GCMS X 11/23/01 A 11/29/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
‘ Data File : C:\HPCHEM\1\DATA\DEC1001\28596.D Vial: 21 Acq On : 11 Dec 2001 6:14 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.599 274 278 291 rBV 279120 681542 10.48% 2.064% 2 11.335 682 685 691 rBV 114540 257829 3.96% 0.781% 3 11.418 691 694 708 rVB 127475 319306 4.91% 0.967% 4 11.666 714 721 740 rBV2 1878290 4934044 75.84% 14.940% 5 15.273 1108 1114 1132 rBV 2834336 5996795 92.18% 18.157%
6 20.552 1683 1689 1714 rBV 2967911 6505554 100.00% 19.698% 7 24.968 2164 2170 2182 rBV2 2550566 5956480 91.56% 18.035% 8 30.054 2718 2724 2733 rBV 311404 643508 9.89% 1.948% 9 33.001 3036 3045 3063 rBV2 1736722 4288977 65.93% 12.986%, 10 33.285 3072 3076 3092 rVB 38707 118235 1.82% 0.358%
11 37.095 3483 3491 3510 rBV2 1164676 3324352 51.10% 10.066%
Sum of corrected areas: 33026622
28596.D GCMS1126.M Fri Dec 14 16:46:42 2001
NYC-WTC_000034913
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NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035651
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000034718
Document with unreadable text from DEP Box 22, folder GCMS X 11/23/01 A 11/29/01.
Filed in the same folder
NYC-WTC_000034719
Gas chromatography-mass spectrometry laboratory analytical data sheet with sample identification numbers, volumetric measurements, drip rates, and final analysis values from…
Filed in the same folder
NYC-WTC_000034722
Gas chromatography-mass spectrometry reference report listing concentrations of volatile organic compounds for sample AD28593.
Filed in the same folder
NYC-WTC_000034727
Calibration results for gas chromatography-mass spectrometry analysis showing detector responses for standard compounds.
Filed in the same folder
NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
Filed in the same folder