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GCMS analysis results sample AD29461, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036469–000036479

Folder label: “GCMS X 12/5/01 A 12/12/01

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Scanned page image, NYC-WTC_000036474
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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\DEC1201\29461.D Vial: 18 Acq On : 12 Dec 2001 7:35 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last ' PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.600 274 278 296 rBV 372995 1034895 13.57% 2.616% 2 11.337 681 685 691 rBV 110767 252998 3.32% 0.640% 3 11.419 691 694 714 rVB 119093 334543 4.39% 0.846% 4 11.667 714 721 740 rBV 2188202 5743703 75.34% 14.520% 5 15.275 1108 1114 1133 rBV 3255842 7053468 92.51% 17.831%

6 20.554 1683 1689 1707 rBV 3523943 7624161 100.00% 19.273% 7 24.970 2164 2170 2183 rBV2 3144757 7111947 93.28% 17.979% 8 25.117 2183 2186 2198 rVB 27526 99717 1.31% 0.252% 9 30.046 2718 2723 2735 rBV 321434 651691 8.55% 1.647% 10 33.012 3039 3046 3060 rBV2 2209173 5379943 70.56% 13.600%

11 37.097 3483 3491 3510 rBV2 1485382 4270945 56.02% 10.797%

Sum of corrected areas: 39558011

29461.D GCMS1126.M Fri Dec 21 12:28:24 2001

NYC-WTC_000036474

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NYC-WTC_000036474Source: NYC Law Department, mirrored locally

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