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GCMS analysis summary, sample AD31403, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31403 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016260–000016271

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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Scanned page image, NYC-WTC_000016265
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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘'Data File : C:\HPCHEM\1\DATA\JAN1502\31403.D Vial: 12 Acq On : 15 Jan 2002 9:43 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.449 258 262 274 rBV 315210 839182 14.69% 2.934% 2 7.587 275 277 292 rVB 41320 158364 2.77% 0.554% 3 11.277 676 679 694 rVB2 17593 59777 1.05% 0.209% 4 11.497 699 703 722 rBV 1674466 4443464 77.78% 15.536% 5 15.096 1089 1095 1114 rBV 2687781 5525607 96.72% 19.320%

6 20.356 1662 1668 1688 rBV 2801808 5713223 100.00% 19.976% 7 24.772 2143 2149 2161 rBV2 2458576 5209333 91.18% 18.214% 8 24.928 2161 2166 2180 rVB 17836 60421 1.06% 0.211% 9 29.849 2697 2702 2708 rBV 356480 707519 12.38% 2.474% 10 32.796 3017 3023 3038 rBV2 1448889 3393125 59.39% 11.864%

11 36.863 3459 3466 3485 rBV 900485 2490505 43.59% 8.708%

Sum of corrected areas: 28600520

31403.D GCMS1126.M Mon Feb 04 15:11:13 2002

NYC-WTC_000016265

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NYC-WTC_000016265Source: NYC Law Department, mirrored locally

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