GCMS comments for sample AD29789 showing no unusual compounds, Jan

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• Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29789.D Vial: 21 Acq On : 15 Dec 2001 10:02 pm Operator: 209 GALOS Sample : gcms scan 12/10 a Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 11.43 0.76 ug/l 208473 1,4.-Dichlorobenzene-d4 11.67

Hit# of 5 Tentati ID MW MolForm CAS# Qual -------------------- ------------------------------------------------ 1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, -(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 53 3 2-Butanol, ,3'-oxybis- 162 C8H1803 054305-61-2 50 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 Abund Scan 696 (11.432 min): 29789.D (-) m/z 59 1 0.00%

45 5000 73 103

39 86 11.20 11.40 11.60 11.80 50 m/z 45.00 52.65% m/z--> 20 30 40 50 60 70 80 90 100 110 12.0 130 140 Abundance #9238: 2-Propanol 1-(2-methoxy-1-methylethoxy)- i

5000 45 103 11.20 11.40 11.60 11.80 73 31 S m/z 103.00 35.49% 130 m/z-->

20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance 46086: 1-Propanol, 2-(2-hydrexypropoxy)- 59 I i 11.20 11.40 11.60 11.80 5000 m/z 73.00 32.02° 31 j 45 I 103

i 75 89 /z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 11.20 11.40 11.60 11.80 m/z 41.05 23.35% 5000 31 I 45 103

134 'm/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

29789.D GCMS1126.M Fri Dec 28 13:24:59 2001 Page 3

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