GCMS analysis comments, sample AD28967, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0701\28967.D Vial: 13 Acq On 8 Dec 2001 2:38 am Operator: 209 GALOS' Sample : 11/29 gc/ms scan Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 11.42 1.13 ug/l 300299 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative/ /ID MW MolForm CAS# Qual ----------------------- --------------------------------------------- 1 2-Propanol, 1-(2- thoxy-l-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3'- ybis- 162 C8H1803 054305-61-2 64 3 2-Propanol, 1-( -methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 2-Yropanol, 1,l'-oxybis- 134 C6H1403 000110-98-5 40 bundance Scan 695 (11.421 min): 28967.D (-) m/z 59.05 1 0.00%

5000 45 103 73 39 85 11.00 11.20 11.40 11.60 11.80 m/z 45.00 45.55% /z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 bundance #9238: 2-Propanol, 1-(2-methoxy-l-methylethoxy)-

5000 45 73 103 11.00 11.20 11.40 11.60 11.80 31 m/z 103.05 36.48% i , 130 m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2d3utanol. 3,3'-oxybis- 59

i 11.00 11.20 11.40 11.60 11.80 5000 31 45 m/z 73 00 28.16% 103

i~ 134 /z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 bundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 11.00 11.20 11.40 11.60 11.80 m/z 41.05 25.61% 5000

31 i 45 73 104 I. 130 111 1 1 I I I /z--> 20 30 40 50 60 70 80 90 .100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

28967.D GCMS1126.M Thu Dec 13 10:22:28 2001 Page 3

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