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GCMS analysis comments, sample AD28967, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.

NYC-WTC_000035607–000035617

Folder label: “GCMS X 11/29/01 A 12/7/01

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Scanned page image, NYC-WTC_000035615
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0701\28967.D Vial: 13 Acq On 8 Dec 2001 2:38 am Operator: 209 GALOS Sample : 11/29 gc/ms scan Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.80 ug/1 213468 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative.-ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2- ethoxy-l-methylet 148 C7H1603 020324-32-7 83 2 2-Butanol, 3,3' xybis- 162 C8H1803 054305-61-2 64 3 2-Propanol, 1 '-oxybis- 134 C6H1403 000110-98-5 56 4 2-Propanol, -(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 idance Scan 686 (11.339 min): 28967.D (-) m/z .59.05 10 .00%

5000 45 73 103

39 11.00 11.20 11.40 11.60 I 85 94 m/z 45.05 46.55% •> 20 30 40 50 60 70 80 90 100 110 120 130 140 :dance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)-

5000 45 73 103 11.00 11.20 11.40 11.60 31 m/z 103.05 34.64% 130 > 20 30 40 50 60 70 80 90 100 110 120 130 140 dance #12859: 2-f3Litanol. 3,3'-oxybis- 59 I ' 11.00 11.20 11.40 11.60 5000 31 I m/z 73.00 31.14% 45 . 103

134 > 20 30 40 50 60 70 80 90 100 110 120 130 140 dance #6087: 2-Propanol, 1,1'-oxybis- 11.00 11.20 11.40 11.60 m/z 41.05 22.64% 31 5000 45 103 89 72 > 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

28967.D GCMS1126.M Thu Dec 13 10:22:24 2001 Page 2

NYC-WTC 000035615

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NYC-WTC_000035615Source: NYC Law Department, mirrored locally

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