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← Document results/DEP Box 22/GCMS X 12/7/01 A 1/2/02
Document / 27 pages

GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036769
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title . : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 12 Ethyl 4-acetylbenzoate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

32.21 20.93 ug/1 43646000 Chrysene-dl2 33.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl 4-acetylbenzoate 192 C11H1203 038430-55-6 16 2 Edulan 1 192 C13H20O 041678-29-9 14 3 1,3-Benzenedi amine , N,N ‘-diethyl- 164 C10H16N2 005857-99-8 14 4 4 (1H) -Pteridi none, 2-amino-7-methyl 177 C7H7N50 013040-58-9 14 Abundance 7 Scan 2959 (32.213 min): 29522.D (-) m/z 177. 0 100.00% 117

149 5000- 121 57 91 340 284

miz-> 74.4ullal — 209 228 247 265 ° 302 323 1*—— 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 I" •' I 396 ■" i ■ 31.80 32.00 32.20 32.40 32.60 m/z 161.05 76.05% Abundance #20691: Ethyl 4-acetylbenzoate 177

147 5000 31.80 32.00 32.20 32.40 32.60 76 104121 m/ z 149 53.20% II l i il p •• 11 11 n । • <<<।...■। | ! I . TT’’ I . | I . I . | ! ! . < ] I I . > | 1T miz-> 40 60 80 1 00 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #20831: Edulan 1 177 i ■ ■ ■ ' i ■ ■ ■ ■ i ■ ' ■ ' i ' ' 31.80 32.00 32.20 32.40 32.60 5000 m/z 164.05 48.96% 133 105 | 159 i I“"I TWTBup 11 • • • p • • • p • • • p • • • p • • • p •" p " • r •" r • • • p •" r' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #13502: 1,3-Benzenediamine, N,N‘-diethyl- 1 9 31.80 32.00 32.20 32.40 32.60 m/z 121.05 32.08% 67 5000

m/z-> J L T‘l‘"‘10—E810"TTTIETTTTTETTETETTTETU‘IETETETETUTTITTTT‘‘‘TT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 —- — — » — 1 1 31.80 32.00 32.20 32.40 32.60

29522.D GCMS1126.M Fri Jan 18 16:49:01 2002 Page 12

NYC-WTC_000036769

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NYC-WTC_000036769Source: NYC Law Department, mirrored locally

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