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← Document results/DEP Box 22/GCMS X 12/7/01 A 1/2/02
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GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036765
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq Ori 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************************** * * ** * ** ******** * * * * * * * Peak Number 8 Benzenemethanol, .alpha.-methy Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

24.01 10.74 ug/1 10934000 Phenanthrene-dl0 24.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Benzenemethanol/ .alpha.-methyl-.al 198 C14H140 000599-67-7 59 2 Azulene, 1,4- methyl-7-(1-methylet 198 C15H18 000489-84-9 50 3 Benzene, ethy phenoxy- 198 C14H140 054852-74-3 46 4 Cyclopropanecarboxylic acid, 3- (2,2 390 C21H20C12O3 051877-74-8 42 Abundance Scan 2065 (24.006 min): 29522.D (-) m/z 183.05 100.00% 183

5000 198 165 —-------- 77 51 103 120 141 , 23.60 23.80 24.00 24.20 24.40 0 36—44—— 4444 4 221 Tr-r- I ’ 250 281 ’ p-n-rpn 327 11'1'11''' I' 355 m/z 198.05 43.69% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #69651: Benzenemethanol, .alpha.-methyl-.alpha.-phenyl- 183 105 __ ----- 5000 - 77 23.60 23.80 24.00 24.20 24.40 165 m/z 165.10 27.27% 121 198 | —TTT HT ' 'I 1 TT‘| 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #22543: Azulene, 1,4-dimethyl-7-(1-methylethyl)- 183 . | 198 23.60 23.80 24.00 24.20 2440 5000 m/ z 77.0.0 17.49%

128.153168 ■> ! I > ! ! i | i < >-T| i , I > | I I [ I | i , > rp-n-q ri i ‘i I ' " ' I ' ' ' ' I ' ' 1 ' I i ■ • ■ • i • • • ■ i • ■ • ■ । r m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #22520: Benzene, ethylphenoxy- . .................. ......... 4 163 23.60 23.80 24.00 24.20 24.40 198 m/z 91.00 16.58% 5000

miz-> 'r 40 51 I ■ I' 60 77 105 ,| I ' ' ' ' I 155 ■ i ■''' i r '' ■ i' ■'' i l ■ ■ • ■ । 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ l • ■ • ■ l ■ -.. AU. 23.60 23.80 24.00 24.20 24.40

29522.D GCMS1126.M Fri Jan 18 16:48:41 2002 Page 8

NYC-WTC_000036765

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NYC-WTC_000036765Source: NYC Law Department, mirrored locally

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