NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\DEC2701\29563.D Vial: 36
. Acq On 28 Dec 2001 11:11 pm Operator: 209 GALOS
Sample GC/MS SCAN 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Dec 29 0:00 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 1359641 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 5190720 20.00 ug/1 -0.03
17) Acenaphthene-dlO 20.57- 164 2533069 20.00 ug/1 -0.01
29) Phenanthrene-diO 24.98 188 3810154 20.00 ug/1 -0.01
38) Chrysene-dl2 33.02 240 2314101 20.00 ug/1 -0.01
44) Perylene-dl2 37.12 264 1398621 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 172793 4.13 ug/mL 0.00
Spiked Amount 5.000 Recovery = 82.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.30 74 510 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 . N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.54 77 185 N.D.
12) Isophorone 13.86 82 188 N.D.
13) bis(2-Chloroethoxy)methane 14.94 93 108 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.34 128 2345 N.D.
16) Hexachlorobutadiene ' 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.27 163 386 N.D.
21) 2,6-Dinitrotoluene 20.28 165 310 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.37 165 172 N.D.
25) Diethylphthalate 22.11 149 2281 N.D.
26) 4-Chlorophenyl-phenylether 0.00 2 04 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29563.D GCMS1126.M Wed Jan 02 09:07:41 2002 Page 1
NYC-WTC_000036714
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