GCMS analysis results for sample AD29523, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12:10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 29 0:58 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1596657 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 6065117 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 2946459 20.00 ug/1 -0.01 29) Phenanthrene-dlO . 24.99 188 4558549 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 2802906 20.00 ug/1 0.00 44) Perylene-dl2 37.13 264 1661524 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 178466 3.56 ug/mL 0.00 Spiked Amount 5.000 Recovery = 71.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.31 74 218 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 . N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.17 77 203 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 . 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1970 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.27 163 521 N.D. 21) 2,6-Dinitrotoluene 20.27 165 306 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.28 165 752 N.D. 25) Diethylphthalate 22.13 149 1812 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29523 .D GCMS1126 .M Tue Jan 08 15:55:08 2002 Page 1

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