Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 9:59 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 ■11.53 152 1138391 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 4523727 20.00 ug/1 0.00 17) Acenaphthene-diO 20.40 164 2265363 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2793732 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 2041896 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 1162077 20.00 ug/1 0.02
System Monitoring Compounds 37) 2,4-DDD 29.89 235 135273 4.22 ug/mL -0.18 Spiked Amount 5.000 Recovery = 84.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 10.52 93 721 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. d 9) Hexachloroethane () .00 117 0 N.D. 11) Nitrobenzene 13.23 77 1022 N.D. 12) Isophorone 13.72 82 459 N.D. 13) bis(2-Chloroethoxy)methane 14.17 93 1156 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 2096 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 18.25 237 340 N.D. 19) 2-Chloronaphthalene 18.19 162 2767 N.D. 20) Dimethylphthalate 20.13 163 7912 N.D. 21) 2,6-Dinitrotoluene 19.96 165 ill N.D. 22) Acenaphthylene 20.05 152 3581 N.D., 23) Acenaphthene 20.41 153 313 N.D. 24) 2,4-Dinitrotoluene 21.15 165 684 N.D. 25) Diethylphthalate 21.91 149 2078 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29466.D GCMS1126.M Wed Jan 09 10:00:13 2002 Page 1
NYC-WTC_000036616
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NYC-WTC_000036162
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Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
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1 shared non-person entities · 1 shared topics · similarity 0.996
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1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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