GCMS analysis summary, sample AD31378, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31378 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016195–000016203

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI502\31378.D Vial: 13 Acq On : 15 Jan 2002 10:42 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 4 14:08 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 760049 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 3018116 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.36 164 1557710 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.78 188 2189893 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1493115 20.00 ug/1 -0.04 44) Perylene-dl2 36.87 264 1029318 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 29.85 235 150311 5.98 ug/mL -0.22 Spiked Amount 5.000 Recovery = 119.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.14 77 178 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.15 128 2220 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.68 165 255 N.D. 25) Diethylphthalate 21.87 149 832 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31378.D GCMS1126.M Mon Feb 04 14:09:39 2002 Page 1

NYC-WTC_000016197

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000016197Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AD31458, Feb 2002 · Box DEP Box 16

NYC-WTC_000018334

Laboratory report documenting GCMS analysis of sample AD31458 conducted on February 13, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999