Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
NYC-WTC_000033911–000033935Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0 8 02\2 8 3 2 7.D Vial: 5 Acq On : 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample : 508 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 17:05 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 1147630 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 4584033 20.00 ug/1 0.00 17) Acenaphthene-diO 20.40 164 2309110 20.00 ug/1 0.00 29) Phenanthrene-dlO 24.81 188 3340495 20.00 ug/1 0.00 38) Chrysene-dl2 32.85 240 2112421 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 1314443 20.00 ug/1 0.02
System Monitoring Compounds 37) 2,4-DDD 29.88 235 163328 4.26 ug/mL -0.19 Spiked Amount 5.000 Recovery = 85.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3) bis(2-Chloroethyl)ether 4) 1,3-Dichlorobenzene 5.13 0.00 0.00 74 93 146 (Z2) 0 N.D. N.D. N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.83 77 N.D. 12) Isophorone 13.41 82 .292 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 932 ' N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 . 0 N.D. 19) 2-Chloronaphthalene 18.19 162 N.D. 20) Dimethylphthalate 20.13 163 /2495 N.D. 21) 2,6-Dinitrotoluene 19.97 165 (324 N.D. 22) Acenaphthylene 19.94 152 \ 186 y N.D. 23) Acenaphthene 0.00 153 N.D. 24) 2,4-Dinitrotoluene 21.15 165 1036 N.D. 25) Diethylphthalate 21.91 14 9 11432 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd _0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 28327.D GCMS1126.M Wed Jan 09 09:03:14 2002 Page 1
NYC-WTC_000033913
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