NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN1602\31458.D Vial: 6
Acq On : 16 Jan 2002 4:32 pm Operator: 209 GALOS
Sample : gc/ms scan 12/27 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 7 8:39 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.50 152 856937 20.00 ug/1 -0.03
10) Naphthalene-d8 15.09 136 3322608 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.36 164 1661481 20.00 ug/1 -0.03
29) Phenanthrene-diO 24.77 188 2265148 20.00 ug/1 -0.03
38) Chrysene-dl2 32.80 240 1237201 20.00 ug/1 -0.04
44) Perylene-dl2 36.86 264 779947 20.00 ug/1 -0.03
System Monitoring Compounds
37) 2,4-DDD 29.85 235 138480 5.33 ug/mL -0.22
Spiked Amount 5.000 Recovery = 106.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.16 74 328 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.15 128 587 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Ac enapht hene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.87 165 262 N.D.
25) Diethylphthalate 21.89 149 292 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
2 7) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31458.D GCMS0103.M Thu Feb 07 08:41:06 2002 Page 1
NYC-WTC_000018336
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