GCMS unknown compounds report, sample AD31459, Feb 2002

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Laboratory report for DEP sample AD31459 identifying unknown compounds and surrogate recovery results from February 13, 2002.

NYC-WTC_000016533–000016542

Folder label: “GCMS X 12/31/01 A 1/18/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1602\31459.D Vial: 15 Acq On : 17 Jan 2002 1:19 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 8:59 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 839083 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 3272852 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.36 164 1645071 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.78 188 2283076 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1459762 20.00 ug/1 -0.04 44) Perylene-dl2 36.87 264 998887 20.00 ug/1 -0.03

System Monitoring Compounds 37) 2,4-DDD 29.85 235 130575 4.98 ug/mL -0.22 Spiked Amount 5.000 Recovery = 99.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. -5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.16 128 501 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.72 165 383 N.D. 25) Diethylphthalate 21.88 149 744 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31459.D GCMS0103.M Thu Feb 07 09:00:11 2002 Page 1

NYC-WTC_000016535

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GCMS analysis results for sample AD31407, Feb 2002 · Box DEP Box 16

NYC-WTC_000018048

Laboratory report documenting GCMS analysis of sample AD31407 conducted on February 13, 2002.

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