NYC-WTC_000018343
Laboratory report documenting GCMS analysis of sample AD31404 conducted on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS analysis results for sample AD31465, Feb 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD31465 conducted on February 11, 2002.
NYC-WTC_000018385–000018394Folder label: “GCMS X 12/27/01 A 1/16/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN1602\31465.D Vial: 28 Acq On : 17 Jan 2002 3:01 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 7 12:23 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.50 152 883470 20.00 ug/1 -0.03 10) Naphthalene-d8 15.09 136 3452572 20.00 ug/1 -0.02 17) Acenaphthene-dl0 20.36 164 1740545 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.77 188 2441893 20.00 ug/1 -0.03 38) Chrysene-dl2 32.80 240 1627782 20.00 ug/1 -0.03 44) Perylene-dl2 36.87 264 1082673 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 29.86 235 133817 4.77 ug/mL -0.21 Spiked Amount 5.000 Recovery = 95.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.16 128 1468 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.73 165 189 N.D. 25) Diethylphthalate 21.88 149 973 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31465.D GCMS0103.M Thu Feb 07 12:24:18 2002 Page 1
NYC-WTC_000018387
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